Chapter NR 439

NR 439.075(2)(c)1.h. h. Basic oxygen process furnaces at iron and steel plants subject to s. NR 440.31.

NR 439.075(2)(c)1.i. i. Incinerators at sewage treatment plants subject to s. NR 440.32.

NR 439.075(2)(c)1.j. j. Dryers at primary copper smelters subject to s. NR 440.33.

NR 439.075(2)(c)1.k. k. Sintering machines at primary zinc smelters subject to s. NR 440.34.

NR 439.075(2)(c)1.L. L. Blast furnaces, dross reverberatory furnaces and sintering machines at primary lead smelters subject to s. NR 440.35.

NR 439.075(2)(c)1.m. m. Thermal dryers and pneumatic coal cleaning equipment at coal preparation plants subject to s. NR 440.42.

NR 439.075(2)(c)1.n. n. Electric arc furnaces and dust handling equipment at ferroalloy production facilities subject to s. NR 440.43.

NR 439.075(2)(c)1.o. o. Electric arc furnaces at steel plants subject to s. NR 440.44.

NR 439.075(2)(c)1.p. p. Electric arc furnaces and argon-oxygen decarburization vessels at steel plants subject to s. NR 440.445.

NR 439.075(2)(c)1.q. q. Recovery furnaces, smelt dissolving tanks and lime kilns at kraft pulp mills subject to s. NR 440.45.

NR 439.075(2)(c)1.r. r. Melting furnaces at glass manufacturing plants subject to s. NR 440.46.

NR 439.075(2)(c)1.s. s. Kilns at lime manufacturing plants subject to s. NR 440.51.

NR 439.075(2)(c)1.t. t. Control devices at metallic mineral processing plants with sources subject to the requirements of s. NR 440.525.

NR 439.075(2)(c)1.u. u. Dryers, calciners and grinders at phosphate rock plants subject to s. NR 440.54.

NR 439.075(2)(c)1.v. v. Ammonium sulfate dryers at ammonium sulfate manufacturing plants subject to s. NR 440.55.

NR 439.075(2)(c)1.w. w. Saturators and blowing stills at asphalt processing and asphalt roofing manufacturing plants subject to s. NR 440.59.

NR 439.075(2)(c)1.x. x. Rotary spun wool fiberglass insulation manufacturing lines at wool fiberglass insulation plants subject to s. NR 440.69.

NR 439.075(2)(c)2. 2. Compliance emission testing for sulfur dioxide is required for fossil fuel fired steam generators subject to s. NR 440.19 or 440.20.

NR 439.075(2)(c)3. 3. Compliance emission testing for volatile organic compounds, including a determination of the overall control efficiency of any control device, is required for the following:

NR 439.075(2)(c)3.a. a. Control devices at facilities subject to the surface coating of metal furniture requirements in s. NR 440.48.

NR 439.075(2)(c)3.b. b. Control devices at facilities subject to the automobile and light-duty truck surface coating requirements in s. NR 440.53.

NR 439.075(2)(c)3.c. c. Control devices at facilities subject to the graphic arts industry requirements in s. NR 440.56.

NR 439.075(2)(c)3.d. d. Control devices at facilities subject to the pressure sensitive tape and label surface coating requirements of s. NR 440.565.

NR 439.075(2)(c)3.e. e. Control devices at facilities subject to the large appliance surface coating requirements in s. NR 440.57.

NR 439.075(2)(c)3.f. f. Control devices at facilities subject to the metal coil surface coating requirements in s. NR 440.58.

NR 439.075(2)(c)3.g. g. Control devices at facilities subject to the beverage can surface coating requirements of s. NR 440.63.

NR 439.075(2)(c)3.h. h. Control devices at bulk gasoline terminals subject to the requirements in s. NR 440.64.

NR 439.075(2)(c)3.i. i. Control devices at facilities subject to the flexible vinyl and urethane coating and printing requirements of s. NR 440.65.

NR 439.075(2)(c)3.j. j. Control devices at synthetic organic chemical manufacturing facilities subject to the requirements of s. NR 440.675, 440.686 or 440.705.

NR 439.075(2)(c)3.k. k. Control devices at facilities subject to the magnetic tape coating requirements of s. NR 440.71.

NR 439.075(2)(c)3.L. L. Control devices at facilities subject to the polymeric coating of supporting substrate requirements of s. NR 440.74.

NR 439.075(2)(c)4. 4. Compliance emission testing for lead is required for grid casting, paste mixing, 3-process operation, lead oxide, lead reclamation and other lead emitting sources at lead acid battery manufacturing plants subject to s. NR 440.52.

NR 439.075(2)(c)5. 5. Compliance emission testing for nitrogen oxides is required for fossil fuel fired steam generators subject to s. NR 440.19 or 440.20.

NR 439.075(2)(c)6. 6. Compliance emission testing for fluorides is required for the following:

NR 439.075(2)(c)6.a. a. Reactors, filters, evaporators and hot wells at wet process phosphoric acid plants subject to s. NR 440.37.

NR 439.075(2)(c)6.b. b. Evaporators, hot wells, acid sumps and cooling tanks at super phosphoric acid plants subject to s. NR 440.38.

NR 439.075(2)(c)6.c. c. Reactors, granulators, dryers, coolers, screens and mills at diammonium phosphate plants subject to s. NR 440.39.

NR 439.075(2)(c)6.d. d. Mixers, curing belts or dens, reactors, granulators, dryers, cookers, screens, mills and facilities which store run-of-pile material at triple superphosphate plants subject to s. NR 440.40.

NR 439.075(2)(c)6.e. e. Storage or curing piles, conveyors, elevators, screens and mills at granular triple superphosphate storage facilities subject to s. NR 440.41.

NR 439.075(3) (3) Testing schedules.

NR 439.075(3)(a) (a) The owner or operator of a direct stationary source which has received a construction permit shall perform the compliance emission tests required under sub. (2) during the initial operating period authorized by the permit.

NR 439.075(3)(b) (b) Unless otherwise required by statute, rule or permit condition, the owner or operator of a direct stationary source which has received an operation permit shall perform the compliance emission tests required under sub. (2) every 24 months as long as the permit remains valid. Each biennial test shall be performed within 90 days of the anniversary date of the issuance of the permit or within 90 days of an alternate date specified by the department.

NR 439.075(3)(c) (c) The owner or operator of a direct stationary source which has received an elective operation permit under s. 285.60 (2) (b), Stats., shall perform the compliance emission tests required under sub. (2) every 24 months as long as the permit remains valid. Each biennial test shall be performed within 90 days of the anniversary date of the issuance of the permit or within 90 days of an alternate date specified by the department.

NR 439.075(4) (4) Exceptions to compliance emission testing requirements.

NR 439.075(4)(a) (a) The following exceptions apply to the testing required under sub. (2) (a) or (c):

NR 439.075(4)(a)1. 1. The department may grant a written waiver of a scheduled test if any of the following applies:

NR 439.075(4)(a)1.a. a. The direct stationary source associated with the emission point subject to the testing requirement will be ceasing operation within one year of a scheduled test.

NR 439.075(4)(a)1.b. b. The most recently completed test results from a test conducted according to the methods and procedures specified in s. NR 439.07 for the direct stationary source demonstrate that the emissions of the air contaminant for which compliance emission testing is required under this section are 50% or less of the applicable emission limitation.

NR 439.075(4)(a)1.c. c. The direct stationary source associated with the emission point subject to the testing requirement has not operated more than 360 hours in the previous 12 month period prior to the scheduled test date.

NR 439.075(4)(a)1.d. d. The most recently completed test, conducted according to the methods and procedures specified in s. NR 439.07, was conducted less than 12 months prior to the date that testing would be required under par. (b).

NR 439.075(4)(a)2. 2. No periodic compliance emission test is required under this section for any affected emission point equipped with a continuous emission monitor for the air contaminants requiring testing if the monitor meets the performance specification requirements of s. NR 439.09.

NR 439.075(4)(a)3. 3. No periodic compliance emission test is required under this section for any affected emission point of a fuel burning installation that only fires natural gas, propane or distillate fuel oil or any combination of these fuels.

NR 439.075(4)(a)4. 4. The department may grant an extension of up to 180 days for compliance emission testing if the owner or operator of a direct stationary source requests an extension, in writing, and can demonstrate that a representative emissions test cannot be performed within the time frames specified in sub. (3) (b).

NR 439.075(4)(a)5. 5. No periodic compliance emission testing for sulfur dioxide emissions is required under this section for any affected emission point which performs periodic fuel sampling and analysis under s. NR 439.085, according to s. NR 439.08.

NR 439.075(4)(b) (b) All requests for waivers under par. (a) shall be submitted in writing for department review and approval at least 60 days prior to the required test date.

NR 439.075 History History: Cr. Register, September, 1987, No. 381, eff. 10-1-87; am. (1) (b) 1. d., Register, April, 1988, No. 388, eff. 5-1-88; am. (1) (d) 1. d., Register, August, 1989, No. 404, eff. 9-1-89; renum. from NR 439.12 and am. (1) (b) 3. f. and (d) 1. b., Register, February, 1990, No. 410 eff. 3-1-90; renum. (1) (b) 3. a. 16) and 17) to be 17) and 16), am. (1) (b) 3. a. 23) and c. 6), Register, July, 1990, No. 415, eff. 8-1-90; renum. (1) (a) to (d), (2) and (3) to be (1) to (4), NR 439.085 and NR 439.095 and am., Register, May, 1992, No. 437, eff. 6-1-92; renum. (2) (c) 1. t. to w. and 3. d. to f. to be (2) (c) 1. u., v., w. and t., and 3. e., f. and d., cr. (2) (c) 3. j., k. and L., Register, May, 1993, No. 449, eff. 6-1-93; am. (3) (a) to (c), (4) (a) 1. c., cr. (4) (a) 1. d., Register, December, 1993, No. 456, eff. 1-1-94; am. (2) (a) 4., Register, June, 1994, No. 462, eff. 7-1-94; am. (2) (a) (intro.), 4., Register, December, 1995, No. 480, eff. 1-1-96; am. (4) (a) 1. (intro.), Register, December, 1996, No. 492, eff. 1-1-97; CR 02-146: cr. (4) (a) 4. and 5. Register October 2003 No. 574, eff. 11-1-03; CR 01-081: am. (2) (b) 1. Register September 2004 No. 585, eff. 10-1-04; CR 07-036: am. (2) (b) 1. Register November 2008 No. 635, eff. 12-1-08; CR 08-114: am. (2) (c) 3. j. Register July 2009 No. 643, eff. 8-1-09; CR 09-020: am. (3) (a) Register January 2010 No. 649, eff. 2-1-10.

NR 439.08 NR 439.08 Methods and procedures for periodic fuel sampling and analysis. The owner or operator of a source required to conduct fuel sampling and analysis under s. NR 439.085 shall use the methods and procedures listed in this section to obtain fuel samples and perform analyses for certain properties and constituents. Alternative methods may be used if approved, in writing, by the department.

NR 439.08(1) (1) Sampling and analysis of coal.

NR 439.08(1)(a) (a) Coal sampling. Coal sampling shall be performed according to ASTM D2234-02, Standard Practice for Collection of a Gross Sample of Coal, incorporated by reference in s. NR 484.10 (33).

NR 439.08(1)(b) (b) Preparing coal for analysis. Preparation of a coal sample for analysis shall be performed according to ASTM D2013-01, Standard Method of Preparing Coal Samples for Analysis, incorporated by reference in s. NR 484.10 (30).

NR 439.08(1)(c) (c) Sulfur content in coal. The sulfur content of a coal sample shall be determined according to ASTM D3177-02, Standard Test Methods for Total Sulfur in the Analysis Sample of Coal and Coke, or ASTM D4239-04a, Standard Test Methods for Sulfur in the Analysis Sample of Coal and Coke Using High Temperature Tube Furnace Combustion Methods, both incorporated by reference in s. NR 484.10 (45) and (53).

NR 439.08(1)(d) (d) Heat content in coal. The heat content of a coal sample shall be determined according to ASTM D5865-04, Standard Test Method for Gross Calorific Value of Coal and Coke, incorporated by reference in s. NR 484.10 (55g).

NR 439.08(1)(e) (e) Ash content in coal. The ash content of a coal sample shall be determined according to ASTM D3174-04, Standard Test Method for Ash in the Analysis Sample of Coal and Coke from Coal, incorporated by reference in s. NR 484.10 (43).

NR 439.08(1)(f) (f) Moisture content in coal. The moisture content of a coal sample shall be determined according to ASTM D3173-02, Standard Test Method for Moisture in the Analysis Sample of Coal and Coke, incorporated by reference in s. NR 484.10 (42).

NR 439.08(1)(g) (g) Ultimate analysis of coal. The ultimate analysis of a coal sample shall be determined according to ASTM D3176-89, Standard Practice for Ultimate Analysis of Coal and Coke, incorporated by reference in s. NR 484.10 (44).

NR 439.08(1)(h) (h) Coal audit samples. The owner or operator of a source shall be required to participate at least once every 6 months in an interlaboratory coal audit program acceptable to the department. The results of the audit shall be reported to the department in the quarterly report on coal quality required under s. NR 439.085 (2) following receipt of the results from the audit program. The results shall comply with quality control and quality assurance procedures submitted by the owner or operator of the source and approved by the department.

NR 439.08(2) (2) Sampling and analysis of liquid fossil fuel.

NR 439.08(2)(a) (a) Liquid fossil fuel sampling. Liquid fossil fuel sampling shall be performed according to ASTM D4057-95, Standard Practice for Manual Sampling of Petroleum and Petroleum Products, or ASTM D4177-95, Standard Practice for Automatic Sampling of Petroleum and Petroleum Products, incorporated by reference in s. NR 484.10 (51) and (52).

NR 439.08(2)(b) (b) Sulfur content in liquid fossil fuel. The sulfur content of a liquid fossil fuel sample shall be determined according to ASTM D129-00, Standard Test Method for Sulfur in Petroleum Products (General Bomb Method), ASTM D1552-03, Standard Test Method for Sulfur in Petroleum Products (High-Temperature Method), or ASTM D4294-03, Standard Test Method for Sulfur in Petroleum Products by Energy-Dispersive X-ray Fluorescence Spectroscopy, incorporated by reference in s. NR 484.10 (3), (25) and (54).

NR 439.08(2)(c) (c) Heat content in liquid fossil fuel. The heat content of a liquid fossil fuel sample shall be determined according to ASTM D240-02, Standard Test Method for Heat of Combustion of Liquid Hydrocarbon Fuels by a Bomb Calorimeter, incorporated by reference in s. NR 484.10 (4).

NR 439.08(3) (3) Sampling and analysis of fuels other than coal and liquid fossil fuel. The owner or operator of a source required by the department to sample and analyze fuel other than coal and liquid fossil fuel shall use methods and procedures approved, in writing, by the department.

NR 439.08 History History: Renum. from NR 439.07 (2) and am., Register, May, 1992, No. 437, eff. 6-1-92; am. (2) (b), Register, May, 1993, No. 449, eff. 6-1-93; am. (1) (a) to (g), (2) (a) to (c), Register, February, 1995, No. 470, eff. 3-1-95; am. (1) (b), (c), (d), (e) and (g), Register, December, 1996, No. 492, eff. 1-1-97; am. (1) (a), (d), (f), (2) (a) and (b), Register, November, 1999, No. 527, eff. 12-1-99; CR 00-175: am. (1) (a) to (f) and (2) (b) Register March 2002 No. 555, eff. 4-1-02; CR 02-146: am. (1) (a) to (d) and (2) (b) and (c) Register October 2003 No. 574, eff. 11-1-03; CR 05-116: am. (1) (c) to (f) and (2) (b) Register November 2006 No. 611, eff. 12-1-06.

NR 439.085 NR 439.085 Periodic fuel sampling and analysis requirements.

NR 439.085(1) (1) General applicability. Effective April 1, 1989, the requirements of this section apply to all owners or operators of sources described in this section, with the following exceptions:

NR 439.085(1)(a) (a) Sources affected by the RACT sulfur limitations in s. NR 418.04, 418.05, 418.06, 418.07 or 418.08.

NR 439.085(1)(b) (b) Sources with approved RACT variances under s. NR 436.05 affected by the sulfur limitations in s. NR 418.025 or 418.03.

NR 439.085(1)(c) (c) Sources which have installed a sulfur dioxide continuous emission monitor that meets the performance specification requirements of s. NR 439.09.

NR 439.085(2) (2) Requirements for coal burning installations. The coal burning rate for an installation shall be based on the maximum permitted capacity. If the permit does not limit the capacity, the total heat input capacity shall be used:

NR 439.085(2)(a) (a) The owner or operator of a coal burning installation which has a coal burning rate equal to or greater than 250,000 tons per year shall sample coal and submit reports on coal quality in the following manner:

NR 439.085(2)(a)1. 1. Perform coal sampling, using the procedures in ASTM D2234/D2234M-03e1, incorporated by reference in s. NR 484.10 (33), which result in data at least as reliable as classification I-B-1, defined in ASTM D2234/D2234M-03e1 as automatic sampling — full stream cut — systematic spacing, and analyze these samples for ash content, sulfur content and heat content according to the applicable methods and procedures in s. NR 439.08 (1).

NR 439.085(2)(a)2. 2. Submit quarterly reports within 30 days following the end of each calendar quarter which include the following information for each day during the calendar quarter:

NR 439.085(2)(a)2.a. a. The total quantity of coal burned expressed in tons.

NR 439.085(2)(a)2.b. b. Average percent of the ash content of the coal burned.

NR 439.085(2)(a)2.c. c. Average percent of the sulfur content of the coal burned.

NR 439.085(2)(a)2.d. d. Average heat content expressed in Btu per pound of the coal burned.

NR 439.085(2)(a)2.e. e. Average sulfur dioxide emission rate in terms of pounds of sulfur dioxide per million Btu heat input from the coal burned.

NR 439.085(2)(b) (b) The owner or operator of a coal burning installation which has a coal burning rate equal to or greater than 100,000 tons per year but less than 250,000 tons per year shall sample coal and submit reports on coal quality in the following manner:

NR 439.085(2)(b)1. 1. Perform coal sampling using the procedures in ASTM D2234/D2234M-03e1, incorporated by reference in s. NR 484.10 (33), which result in data at least as reliable as classification I-C-2, defined in ASTM D2234/D2234M-03e1 as automatic sampling — part stream cut — random spacing, and analyze these samples for ash content, sulfur content and heat content according to the applicable methods and procedures in s. NR 439.08 (1).

NR 439.085(2)(b)2. 2. Submit quarterly reports within 30 days following the end of each calendar quarter which include the following information for each week during the calendar quarter: