The consent of the Attorney General will be requested for the incorporation by reference of
— ASTM D8174-18 Standard Test Method for Finite Flash Point Determination of Liquid Wastes by Small Scale Closed Cup Tester, incorporated by reference for s. NR 661.0021 (1). This test method covers the procedure for a flash point test, within the range of –20 to 70 °C, of liquid wastes using a small-scale closed cup tester. This test method is not applicable for liquid waste that forms a surface film. — ASTM D8175-18, Standard Test Method for Finite Flash Point Determination of Liquid Wastes by Pensky-Martens Closed Cup Tester, incorporated by reference for s. NR 661.0021 (1). This test method covers the procedure for a finite flash point test, within the range of 20 to 70 °C, of liquid wastes using a manual or automated Pensky-Martens closed cup tester. This test method contains two procedures and is applicable to liquid waste, liquid phase(s) of multi-phase waste, liquid waste with suspended solids, or liquid waste that tends to form a surface film under test conditions. — ASTM E681-85, Standard Test Method for Concentration Limits of Flammability of Chemicals (Vapors and gases), incorporated by reference for s. NR 661.0021 (1). This test method is used to determine the upper and lower concentration limits of flammability for chemicals having sufficient vapor pressure to form flammable mixtures with air. — Method 1010B, December 2018, incorporated by reference for s. NR 661.0021. Method 1010B lists the Pensky-Martens flash point methods, which are ASTM Standards D93–79, D93–80, and D8175–18. — Method 1020C, December 2018, incorporated by reference for s. NR 661.0021. lists the Setaflash (small-scale) closed cup flash point methods, which are the ASTM Standards D3278–78 and D8174–18. ASTM D8174–18 is a test method to determine the flash point of liquid wastes using a small-scale (Setaflash) apparatus. ASTM D8175–18 is a test method used to determine the flash point of liquid wastes using a Pensky-Martens apparatus. — Method 0011, August 2018 and Update I, incorporated by reference for ch. NR 666 Appendix IX. Method 0011 is a method for collection of selected ketones and aldehydes from an emission source. — Method 0023A, August 2018 and Update II, incorporated by reference for s. NR 666.104 and ch. NR 666 Appendix IX. Method 0023A is a method for collection of polychlorinated dibenzo-p-dioxins and polychlorinated dibenzofuran from an emission source. — Method 0051,Revision 1, August 2018 , incorporated by reference for s. NR 666.107 and ch. NR 666 Appendix IX. Method 0051 is a method for collection of hydrogen chloride and chlorine in stack gas emission samples from hazardous waste incinerators and combustors. — Method 1330A, Extraction Procedure for Oily Wastes, dated July 1992 and in Update I, incorporation by reference approved for appendix IX to part 261.
— Method 9071B, n-Hexane Extractable Material (HEM) for Sludge, Sediment, and Solid Samples, dated April 1998 and in Update IIIA, incorporated by reference for ch. 661 Appendix IX. This method may be used to quantify low concentrations of oil and grease in soil, sediments, sludges, and other solid materials amenable to chemical drying and solvent extraction with n-hexane. Method 9071 employs n-hexane as the extraction solvent with Soxhlet extraction and the results of this method are termed “n-hexane extractable material (HEM).” “HEM” is used synonymously with “oil and grease. Method 9071 is suitable for extracting relatively non-volatile hydrocarbons, vegetable oils, animal fats, waxes, soaps, greases, biological lipids, and related materials and is not recommended for measuring materials that volatilize at temperatures below 85 degrees Celsius. Steel Tank Institute, “Standards for Dual Wall Underground Storage Tanks,” 2006, incorporated by reference for s. NR 661.0193 (4). These standard addresses underground double containment (atmospheric-type) vessels with built-in interstitial monitoring capability for the purpose of giving advance notice to avoid environmental contamination. — Method 1311, July 1992, and Update I, incorporated by reference for ss. NR 661.0024, 668.07, 668.40 and 661 Appendix IX. This method is used for assessing the presence of an ignitable liquid for wastes that do not yield a free liquid phase using Method 9095 (i.e., Paint Filter Liquids Test or PFLT). RULE TEXT+
Section 1 NR 660.11 (1) and (Note) are amended to read:
NR 660.11 (1) This section is adopted under ss. 227.21 (2) (b) and 291.05, Stats., to incorporate by reference testing, monitoring, and other technical standards, established by the federal government and technical societies and organizations, to which reference is made under chs. NR 660 to 670 679. Some materials Materials that are incorporated by reference under other references are hereby incorporated by reference and made a part of this subsection. Note: Copies of these materials are available for inspection in the offices office of the Department of Natural Resources, Madison, Wisconsin, the Legislative Reference Bureau, or may be obtained for personal use at the addresses noted.
Section 2 NR 660.11 (2), (3), (4), (5), (6) and (7) are repealed and recreated to read:
NR 660.11 (2) The following materials are available for purchase from the American Society for Testing and Materials, 100 Barr Harbor Drive, P.O. Box C700, West Conshohocken, PA 19428–2959, (877) 909-2786, www.astm.org.: (a) ASTM D93–79, Standard Test Methods for Flash Point by Pensky-Martens Closed Cup Tester, incorporated by reference for s. NR 661.0021. (b) ASTM D93–80, Standard Test Methods for Flash Point by Pensky-Martens Closed Cup Tester, incorporated by reference for s. NR 661.0021. (c) ASTM D1946–82, Standard Method for Analysis of Reformed Gas by Gas Chromatography, incorporated by reference for ss. NR 664.1033 and 665.1033. (d) ASTM D2267–88, Standard Test Method for Aromatics in Light Naphthas and Aviation Gasolines by Gas Chromatography, incorporated by reference for s. NR 664.1063. (e) ASTM D2382–83, Standard Test Method for Heat of Combustion of Hydrocarbon Fuels by Bomb Calorimeter (High-Precision Method), incorporated by reference for ss. NR 664.1033 and 665.1033. (f) ASTM D2879–92, Standard Test Method for Vapor Pressure—Temperature Relationship and Initial Decomposition Temperature of Liquids by Isoteniscope, incorporated by reference for s. NR 665.1084. (g) ASTM D3278–78, Standard Test Methods for Flash Point for Liquids by Setaflash Closed Tester, incorporated by reference for s. NR 661.0021 (1). (h) ASTM D8174-18, Standard Test Method for Finite Flash Point Determination of Liquid Wastes by Small Scale Closed Cup Tester, incorporated by reference for s. NR 661.0021 (1). (i) ASTM D8175-18, Standard Test Method for Finite Flash Point Determination of Liquid Wastes by Pensky-Martens Closed Cup Tester, incorporated by reference for s. NR 661.0021 (1). (j) ASTM E168–88, Standard Practices for General Techniques of Infrared Quantitative Analysis, incorporated by reference for s. NR 664.1063. (k) ASTM E169–87, Standard Practices for General Techniques of Ultraviolet-Visible Quantitative Analysis, incorporated by reference for s. NR 664.1063. (L) ASTM E260–85, Standard Practice for Packed Column Gas Chromatography, incorporated by reference for s. NR 664.1063. (m) ASTM E681-85, Standard Test Method for Concentration Limits of Flammability of Chemicals (Vapors and gases), incorporated by reference for s. NR 661.0021 (1). (n) ASTM E926–88, Standard Test Methods for Preparing Refuse-Derived Fuel (RDF) Samples for Analyses of Metals, Test Method C—Bomb, Acid Digestion Method.
(o) ASTM D140-70, Standard Practice for Sampling Bituminous Materials, incorporated by reference for ch. NR 661 Appendix I. (p) ASTM D346-75, Standard Practice for Collection and Preparation of Coke Samples for Laboratory Analysis, incorporated by reference for ch. NR 661 Appendix I. (q) ASTM D420-69, Guide to Site Characterization for Engineering, Design, and Construction Purposes, incorporated by reference for ch. NR 661 Appendix I. (r) ASTM D1452-65, Standard Practice for Soil Investigation and Sampling by Auger Borings, incorporated by reference for ch. NR 661 Appendix I. (s) ASTM D2234-76, Standard Practice for Collection of a Gross Sample of Coal, incorporated by reference for ch. NR 661 Appendix I. (t) ASTM D2879-86, Standard Test Method for Vapor Pressure—Temperature Relationship and Initial Decomposition Temperature of Liquids by Isoteniscope, incorporated by reference for ch. NR 664 and subch. BB of ch. NR 665. (u) ASTM G21-70 (1984a), Standard Practice for Determining Resistance of Synthetic Polymer Materials to Fungi, incorporated by reference for ch. NR 664 and subch. N of ch. NR 665. (v) ASTM G22-76 (1984b), Standard Practice for Determining Resistance of Plastics to Bacteria, incorporated by reference for ch. NR 664 and subch. N of ch. NR 665. (3) The following materials are available for purchase from the National Technical Information Service, 5285 Port Royal Road, Springfield, VA 22161; or for purchase from the Superintendent of Documents, U.S. Government Printing Office, Washington, DC 20402, (202) 512–1800:
(a) APTI Course 415: Control of Gaseous Emissions, EPA Publication EPA–450/2–81– 005, December 1981, incorporated by reference for ss. NR 664.1035, 665.1035, 670.024, and 670.025. (b) Screening Procedures for Estimating the Air Quality Impact of Stationary Sources, Revised, October 1992, EPA Publication No. EPA–450/R–92–019, incorporated by reference for ch. NR 666 Appendix IX. (c) The following methods as published in the test methods compendium known as “Test Methods for Evaluating Solid Waste, Physical/Chemical Methods,” EPA Publication SW–846, Third Edition:
1. Method 0011, Revision 1, August 2018, incorporated by reference for ch. NR 666 Appendix IX.
