NR 466.09(2)(a)(a) For the purpose of meeting the requirements of s. NR 466.06, the organic HAP weight-fraction of each ink, coating, varnish, adhesive, primer, solvent and other material used in a publication rotogravure affected source shall be determined in accordance with one of the following procedures: NR 466.09(2)(a)1.1. Use Method 311 in 40 CFR Part 63, Appendix A, incorporated by reference in s. NR 484.04, or obtain the results of a Method 311 test performed by the manufacturer of the material. If the organic HAP weight-fraction for any material cannot be determined using Method 311, the owner or operator shall submit an alternate method to the U.S. environmental protection agency for approval by the administrator. The recovery efficiency of the proposed technique shall be determined for all of the target organic HAP and a correction factor, if necessary, shall be determined and applied. NR 466.09(2)(a)2.2. Determine the volatile matter content of the material in accordance with sub. (3) (a), and use this value for the organic HAP content for all compliance purposes. NR 466.09(2)(a)3.3. Use formulation data provided by the manufacturer of the material on a CPDS if the manufacturer has done both of the following: NR 466.09(2)(a)3.a.a. Included in the organic HAP content determination all HAP present at a level greater than 0.1% in any raw material used, weighted by the mass fraction of each raw material used in the material. NR 466.09(2)(a)3.b.b. Determined the HAP content of each raw material present in the formulation by Method 311 in 40 CFR Part 63, Appendix A, incorporated by reference in s. NR 484.04, or by an alternate method approved by the administrator, or by reliance on a CPDS from a raw material supplier prepared in accordance with subpar. a. NR 466.09(2)(b)(b) For the purpose of meeting the requirements of s. NR 466.07, the organic HAP weight-fraction of each ink, coating, varnish, adhesive, primer, solvent, thinner, reducer, diluent and other material used in a product and packaging rotogravure or wide-web flexographic affected source shall be determined in accordance with one of the following procedures: NR 466.09(2)(b)1.1. Use Method 311 in 40 CFR Part 63, Appendix A, incorporated by reference in s. NR 484.04, or obtain the results of a Method 311 test performed by the manufacturer of the material. If the organic HAP weight-fraction for any material cannot be determined using Method 311, the owner or operator shall submit an alternate method to the U.S. environmental protection agency for approval by the administrator. The recovery efficiency of the proposed technique shall be determined for all of the target organic HAP and a correction factor, if necessary, shall be determined and applied. NR 466.09(2)(b)2.2. Determine the volatile matter content of the material in accordance with sub. (3) (b), and use this value for the organic HAP content for all compliance purposes. NR 466.09(2)(b)3.3. Use formulation data provided by the manufacturer of the material on a CPDS if the manufacturer has done both of the following: NR 466.09(2)(b)3.a.a. Included in the organic HAP content determination all organic HAP present at a level greater than 0.1% in any raw material used, weighted by the mass fraction of each raw material used in the material. NR 466.09(2)(b)3.b.b. Determined the organic HAP content of each raw material present in the formulation by Method 311 in 40 CFR Part 63, Appendix A, incorporated by reference in s. NR 484.04, or by an alternate method approved by the administrator, or by reliance on a CPDS from a raw material supplier prepared in accordance with subpar. a. NR 466.09(2)(c)(c) In the event of any inconsistency between the organic HAP content of a material determined using test data from Method 311 in 40 CFR Part 63, Appendix A, incorporated by reference in s. NR 484.04, and the organic HAP content of the same material determined using formulation data as allowed under par. (a) 3. or (b) 3., the Method 311 test data shall govern, unless after consultation, an owner or operator demonstrates to the satisfaction of the department that the formulation data are correct. NR 466.09(3)(a)(a) For the purpose of meeting the requirements of s. NR 466.06, the volatile matter weight-fraction of each ink, coating, varnish, adhesive, primer, solvent, diluent, reducer, thinner and other material used in a publication rotogravure affected source shall be determined in accordance with one of the following procedures: NR 466.09(3)(a)1.1. Use Method 24A in 40 CFR Part 60, Appendix A, incorporated by reference in s. NR 484.04, or obtain the results of a Method 24A test performed by the manufacturer of the material. If the volatile matter weight-fraction for any material cannot be determined using Method 24A, the owner or operator shall submit an alternate method to the U.S. environmental protection agency for approval by the administrator. NR 466.09(3)(a)2.2. Use formulation data, or volatile matter content data provided by material suppliers. NR 466.09(3)(b)(b) For the purpose of meeting the requirements of s. NR 466.07, the volatile matter and solids weight-fraction of each ink, coating, varnish, adhesive, primer, solvent, diluent, reducer, thinner and other material used in a product and packaging rotogravure or wide-web flexographic affected source shall be determined in accordance with one of the following procedures: NR 466.09(3)(b)1.1. Use Method 24 in 40 CFR Part 60, Appendix A, incorporated by reference in s. NR 484.04, or obtain the results of a Method 24 test performed by the manufacturer of the material. If the volatile matter or solids weight-fraction for any material cannot be determined using Method 24, the owner or operator shall submit an alternate method to the U.S. environmental protection agency for approval by the administrator. NR 466.09(3)(b)2.2. Use formulation data, or volatile matter and solids content data provided by material suppliers. NR 466.09(3)(c)(c) In the event of any inconsistency between the volatile matter or solids content of a material determined using formulation data as allowed under par. (a) 2. or (b) 2., and the volatile matter or solids content of the same material using the results of Method 24 or 24A in 40 CFR Part 60, Appendix A, incorporated by reference in s. NR 484.04, the applicable test method shall govern, unless after consultation, the owner or operator can demonstrate to the satisfaction of the department that the formulation data are correct. NR 466.09(4)(4) Control device destruction efficiency. A performance test of a control device to determine destruction efficiency for the purpose of meeting the requirements of ss. NR 466.06 and 466.07, shall be conducted by the owner or operator in accordance with the following requirements: NR 466.09(4)(a)(a) An initial performance test to establish the destruction efficiency of an oxidizer and the associated combustion zone temperature for a thermal oxidizer and the associated catalyst bed inlet temperature for a catalytic oxidizer shall be conducted and the data reduced in accordance with the following reference methods and procedure: