NR 661.1034(4)(a)2.2. For material generated on-site, the grab samples shall be collected at a point before the material is exposed to the atmosphere such as in an enclosed pipe or other closed system that is used to transfer the material after generation to the first affected distillation, fractionation, thin-film evaporation, solvent extraction, or air or steam stripping operation. For material generated off-site, the grab samples shall be collected at the inlet to the first material management unit that receives the material, provided the material has been transferred to the facility in a closed system such as a tank truck and the material is not diluted or mixed with other material.
NR 661.1034(4)(a)3.3. Each sample shall be analyzed and the total organic concentration of the sample shall be computed using Method 9060A of “Test Methods for Evaluating Solid Waste, Physical/Chemical Methods,” EPA Publication SW-846, incorporated by reference in s. NR 660.11, or analyzed for its individual organic constituents.
NR 661.1034(4)(a)4.4. The arithmetic mean of the results of the analyses of the 4 samples shall apply for each material stream managed in the unit in determining the time-weighted, annual average total organic concentration of the material. The time-weighted average shall be calculated using the annual quantity of each material stream processed and the mean organic concentration of each material stream managed in the unit.
NR 661.1034(4)(b)(b) Using knowledge of the material to determine that its total organic concentration is less than 10 ppmw. Documentation of the material determination is required. Examples of documentation that shall be used to support a determination under this provision include production process information documenting that no organic compounds are used, information that the material is generated by a process that is identical to a process at the same or another facility that has previously been demonstrated by direct measurement to generate a material stream having a total organic content less than 10 ppmw, or prior speciation analysis results on the same material stream where it can also be documented that no process changes have occurred since that analysis that could affect the material total organic concentration.
NR 661.1034(5)(5)The determination that distillation, fractionation, thin-film evaporation, solvent extraction, or air or steam stripping operations manage hazardous secondary material with time-weighted, annual average total organic concentrations less than 10 ppmw shall be made by the remanufacturer or other person in accordance with all the following:
NR 661.1034(5)(a)(a) By the effective date that the facility becomes subject to the provisions of this subchapter or by the date when the material is first managed in a hazardous secondary material management unit, whichever is later.
NR 661.1034(5)(b)(b) Annually for continuously generated material, or whenever there is a change in the material being managed or a change in the process that generates or treats the material.
NR 661.1034(6)(6)When a remanufacturer or other person that stores or treats the hazardous secondary material and the department do not agree on whether a distillation, fractionation, thin-film evaporation, solvent extraction, or air or steam stripping operation manages a hazardous secondary material with organic concentrations of at least 10 ppmw based on knowledge of the material, the dispute may be resolved by using direct measurement as specified in sub. (4) (a).
NR 661.1034 HistoryHistory: CR 19-082: cr. Register August 2020 No. 776, eff. 9-1-20; correction in (1), (2) (a), (4) (a) 3. made under s. 35.17, Stats., Register August 2020 No. 776.
NR 661.1035NR 661.1035Recordkeeping requirements.
NR 661.1035(1)(1)
NR 661.1035(1)(a)(a) A remanufacturer or other person that stores or treats the hazardous secondary material subject to the provisions of this subchapter shall comply with the recordkeeping requirements of this section.
NR 661.1035(1)(b)(b) A remanufacturer or other person that stores or treats the hazardous secondary material of more than one hazardous secondary material management unit subject to the provisions of this subchapter may comply with the recordkeeping requirements for these hazardous secondary material management units in one recordkeeping system if the system identifies each record by each hazardous secondary material management unit.
NR 661.1035(2)(2)A remanufacturer or other person that stores or treats the hazardous secondary material shall keep all of the following records on-site:
NR 661.1035(2)(a)(a) For facilities that comply with the provisions specified in s. NR 661.1033 (1), an implementation schedule that includes dates by which the closed-vent system and control device will be installed and in operation. The schedule shall also include a rationale of why the installation cannot be completed at an earlier date. The implementation schedule shall be kept on-site at the facility by the effective date that the facility becomes subject to the provisions of this subchapter.
NR 661.1035(2)(b)(b) Up-to-date documentation of compliance with the process vent standards specified in s. NR 661.1032, including all of the following:
NR 661.1035(2)(b)1.1. Information and data identifying all affected process vents, annual throughput and operating hours of each affected unit, estimated emission rates for each affected vent and for the overall facility, and the approximate location within the facility of each affected unit, such as identifying the hazardous secondary material management units on a facility plot plan.
NR 661.1035(2)(b)2.2. Information and data supporting determinations of vent emissions and emission reductions achieved by add-on control devices based on engineering calculations or source tests. For the purpose of determining compliance, determinations of vent emissions and emission reductions shall be made using operating parameter values, such as temperatures, flow rates, or vent stream organic compounds and concentrations, that represent the conditions that result in maximum organic emissions, such as when the hazardous secondary material management unit is operating at the highest load or capacity level reasonably expected to occur. If the remanufacturer or other person that stores or treats the hazardous secondary material takes any action, such as managing a material of different composition or increasing operating hours of affected hazardous secondary material management units, that would result in an increase in total organic emissions from affected process vents at the facility, then a new determination is required.
NR 661.1035(2)(c)(c) When a remanufacturer or other person that stores or treats the hazardous secondary material chooses to use test data to determine the organic removal efficiency or total organic compound concentration achieved by the control device, a performance test plan shall be developed and include all of the following:
NR 661.1035(2)(c)1.1. A description of how it is determined that the planned test is going to be conducted when the hazardous secondary material management unit is operating at the highest load or capacity level reasonably expected to occur. This shall include the estimated or design flow rate and organic content of each vent stream and define the acceptable operating ranges of key process and control device parameters during the test program.
NR 661.1035(2)(c)2.2. A detailed engineering description of the closed-vent system and control device including all of the following:
NR 661.1035(2)(c)2.a.a. Manufacturer’s name and model number of control device.
NR 661.1035(2)(c)2.b.b. Type of control device.
NR 661.1035(2)(c)2.c.c. Dimensions of the control device.
NR 661.1035(2)(c)2.d.d. Capacity.
NR 661.1035(2)(c)2.e.e. Construction materials.
NR 661.1035(2)(c)3.3. A detailed description of sampling and monitoring procedures, including sampling and monitoring locations in the system, the equipment to be used, sampling and monitoring frequency, and planned analytical procedures for sample analysis.
NR 661.1035(2)(d)(d) Documentation of compliance with s. NR 661.1033 including all of the following information:
NR 661.1035(2)(d)1.1. A list of all information references and sources used in preparing the documentation.